Water is essencitial factor to survive in nature, in the era of progressing and developing stage of industries there is lots of adverse effect of it. Industrial waste effluent directly dumped into water sources like river ,ponds and canals which is drink by human beings and invite dangerous and incurable disease like asthama,cancer of skin, particularly excess level of nickel in drinking water responsible for cancer of skin. Dowex M 4195 resin , Bis(2-pyridylmethyl) amine functional group have capacity to remove heavy metal ions from aqueous solutions. Physical, chemical and liquid-phase adsorption characterizations of the Resin was done following standard procedures. Studies on the removal of Ni(II) ion was attempted by varying pH of the metal ion solution, initial concentration of solution in batch mode.